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<article article-type="research-article" dtd-version="1.3" xmlns:mml="http://www.w3.org/1998/Math/MathML" xmlns:xlink="http://www.w3.org/1999/xlink" xmlns:xsi="http://www.w3.org/2001/XMLSchema-instance" xml:lang="ru"><front><journal-meta><journal-id journal-id-type="publisher-id">vsgiu</journal-id><journal-title-group><journal-title xml:lang="ru">Вестник Сибирского государственного индустриального университета</journal-title><trans-title-group xml:lang="en"><trans-title>Bulletin of the Siberian State Industrial University</trans-title></trans-title-group></journal-title-group><issn pub-type="ppub">2304 - 4497</issn><issn pub-type="epub">2307-1710</issn><publisher><publisher-name>Федеральное государственное бюджетное образовательное учреждение высшего образования "Сибирский государственный индустриальный университет"</publisher-name></publisher></journal-meta><article-meta><article-id pub-id-type="doi">10.57070/2304-4497-2025-3(53)-17-26</article-id><article-id custom-type="elpub" pub-id-type="custom">vsgiu-711</article-id><article-categories><subj-group subj-group-type="heading"><subject>Research Article</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="ru"><subject>Раздел 1. Физика конденсированного состояния</subject></subj-group><subj-group subj-group-type="section-heading" xml:lang="en"><subject>Section 1. Condensed Matter Physics</subject></subj-group></article-categories><title-group><article-title>РОЛЬ ВЫСОКОТЕМПЕРАТУРНОГО ОТПУСКА В ФОРМИРОВАНИИ СТРУКТУРНО-ФАЗОВЫХ СОСТОЯНИЙ ПЛАЗМЕННО НАПЛАВЛЕННОЙ МОЛИБДЕНОВОЙ БЫСТРОРЕЖУЩЕЙ СТАЛИ</article-title><trans-title-group xml:lang="en"><trans-title>ROLE OF HIGH-TEMPERATURE TEMPERING IN FORMATION OF STRUCTURAL-PHASE STATES OF PLASMA-DEPOSITED MOLYBDENUM HIGH-SPEED STEEL</trans-title></trans-title-group></title-group><contrib-group><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0002-5147-5343</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Громов</surname><given-names>Виктор Евгеньевич</given-names></name><name name-style="western" xml:lang="en"><surname>Gromov</surname><given-names>Viktor E.</given-names></name></name-alternatives><bio xml:lang="ru"><p>д.ф.-м.н., профессор, заведующий кафедрой естественнонаучных дисциплин им. проф. В.М. Финкеля</p></bio><bio xml:lang="en"><p>Dr. Sci. (Phys.-Math.), Prof., Head of the Chair of Science named after V.M. Finkel’</p></bio><email xlink:type="simple">gromov@physics.sibsiu.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0001-8022-7958</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Иванов</surname><given-names>Юрий Федорович</given-names></name><name name-style="western" xml:lang="en"><surname>Ivanov</surname><given-names>Yuri F.</given-names></name></name-alternatives><bio xml:lang="ru"><p>д.ф.-м.н., профессор, главный научный сотрудник</p></bio><bio xml:lang="en"><p>Dr. Sci. (Phys.-Math.), Chief Researcher</p></bio><email xlink:type="simple">yufi55@mail.ru</email><xref ref-type="aff" rid="aff-2"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0003-4487-3260</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Баклушина</surname><given-names>Ирина Викторовна</given-names></name><name name-style="western" xml:lang="en"><surname>Baklushina</surname><given-names>Irina V.</given-names></name></name-alternatives><bio xml:lang="ru"><p>старший преподаватель, заместитель директора Института открытого образования</p></bio><bio xml:lang="en"><p>Senior Lecturer, Deputy Director of the Institute of Open Education</p></bio><email xlink:type="simple">baklushina_iv@sibsiu.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0009-0009-8160-7827</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Чапайкин</surname><given-names>Александр Сергеевич</given-names></name><name name-style="western" xml:lang="en"><surname>Chapaykin</surname><given-names>Aleksandr S.</given-names></name></name-alternatives><bio xml:lang="ru"><p>аспирант</p></bio><bio xml:lang="en"><p>Postgraduate Student</p></bio><email xlink:type="simple">thapajkin.s@yandex.ru</email><xref ref-type="aff" rid="aff-1"/></contrib><contrib contrib-type="author" corresp="yes"><contrib-id contrib-id-type="orcid">https://orcid.org/0000-0002-3394-7941</contrib-id><name-alternatives><name name-style="eastern" xml:lang="ru"><surname>Крюков</surname><given-names>Роман Евгеньевич</given-names></name><name name-style="western" xml:lang="en"><surname>Kryukov</surname><given-names>Roman E.</given-names></name></name-alternatives><bio xml:lang="ru"><p>д.т.н., доцент, профессор кафедры механики и машиностроения</p></bio><bio xml:lang="en"><p>Dr. Sci. (Eng.), Associate Professor, Professor of the Department of Mechanics and Mechanical Engineering</p></bio><email xlink:type="simple">rek_nzrmk@mail.ru</email><xref ref-type="aff" rid="aff-3"/></contrib></contrib-group><aff-alternatives id="aff-1"><aff xml:lang="ru"><institution>Сибирский государственный индустриальный университет</institution><country>Россия</country></aff><aff xml:lang="en"><institution>Siberian State Industrial University</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-2"><aff xml:lang="ru"><institution>Институт сильноточной электроники СО РАН</institution><country>Russian Federation</country></aff><aff xml:lang="en"><institution>Institute of High-Current Electronics SB RAS</institution><country>Russian Federation</country></aff></aff-alternatives><aff-alternatives id="aff-3"><aff xml:lang="ru"><institution>Сибирского государственного индустриального университета</institution><country>Russian Federation</country></aff><aff xml:lang="en"><institution>Siberian State Industrial University</institution><country>Russian Federation</country></aff></aff-alternatives><pub-date pub-type="collection"><year>2025</year></pub-date><pub-date pub-type="epub"><day>30</day><month>09</month><year>2025</year></pub-date><volume>0</volume><issue>3</issue><fpage>17</fpage><lpage>26</lpage><permissions><copyright-statement>Copyright &amp;#x00A9; Громов В., Иванов Ю., Баклушина И., Чапайкин А., Крюков Р., 2025</copyright-statement><copyright-year>2025</copyright-year><copyright-holder xml:lang="ru">Громов В., Иванов Ю., Баклушина И., Чапайкин А., Крюков Р.</copyright-holder><copyright-holder xml:lang="en">Gromov V., Ivanov Y., Baklushina I., Chapaykin A., Kryukov R.</copyright-holder><license xml:lang="ru" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>Данная работа распространяется под лицензией Creative Commons Attribution 4.0.</license-p></license><license xml:lang="en" license-type="creative-commons-attribution" xlink:href="https://creativecommons.org/licenses/by/4.0/" xlink:type="simple"><license-p>This work is licensed under a Creative Commons Attribution 4.0 License.</license-p></license></permissions><self-uri xlink:href="https://vestnik.sibsiu.ru/jour/article/view/711">https://vestnik.sibsiu.ru/jour/article/view/711</self-uri><abstract><p>Технологией плазменной наплавки в среде азота на стали марки 30ХГСА порошковой проволокой системы MoCrCoC диаметром 4 мм сформирован наплавленный слой толщиной примерно 9 ‒ 10 мм. В качестве плазмообразующего газа использовали аргон высшего сорта. Методами современного физического материаловедения изучены структурно-фазовые состояния и дефектная субструктура поверхности плазменно наплавленного слоя в среде азота быстрорежущей молибденовой сталью на подложку, подвергнутого двукратному отпуску при температуре 560 ‒ 580 °С в течение 1 ч. Показано, что наплавленный слой имеет поликристаллическую структуру и содержит прослойки эвтектики. Выявлено формирование в наплавленном слое многофазной структуры, представленной α-фазой (твердый раствор на основе ОЦК кристаллической решетки Fe), γ-фазой (твердый раствор на основе ГЦК кристаллической решетки Fe), карбидов сложного состава Me23C6 и Me6C, железа Fe3C и хрома Cr3C2. Установлено, что отпуск наплавленного слоя не приводит к изменению морфологии структуры, сформированной зернами эвтектики и твердого раствора на основе α-железа (ОЦК кристаллическая решетка). Основными фазами являются α-Fe (85 мас. %) и карбиды сложного состава Me23C6 (9 мас. %) и Me6C (6 мас. %), формирующие зерна эвтектики. Установлено, что отпуск наплавленного слоя сопровождается допревращением остаточного аустенита с образованием по границам кристаллов мартенсита наноразмерных частиц карбидов железа и хрома. Вдоль межфазных границ раздела и в объеме пластин карбидной фазы зерен эвтектики выявлены микротрещины, которые могут инициировать разрушение материала наплавленного слоя при эксплуатации.</p></abstract><trans-abstract xml:lang="en"><p>The technology of plasma surfacing in nitrogen on 30HGSA grade steel with a powder wire of the MoCrCoC system with a diameter of 4 mm formed a deposited layer with a thickness of approximately 9 ‒ 10 mm Argon of the highest grade was used as the plasma-forming gas. The structural and phase states and defective substructure of the surface of a plasma-deposited layer in a nitrogen medium with high-speed molybdenum steel on a substrate subjected to double tempering at a temperature of 560 ‒ 580 °C for 1 hour have been studied by methods of modern physical materials science. It is shown that the deposited layer has a polycrystalline structure and contains layers of eutectic. The formation of a multiphase structure in the deposited layer was revealed, represented by an α-phase (solid solution based on the BCC crystal lattice Fe), a γ-phase (solid solution based on the FCC crystal lattice Fe), carbides of complex composition Me23C6 and Me6C, iron carbides Fe3C and chromium Cr3C2. It was established that tempering of the deposited layer does not lead to a change in the morphology of the structure formed by grains of eutectic and a solid solution based on α-iron (BCC crystal lattice). The main phases are α-Fe (85 wt. %) and carbides of complex composition Me23C6 (9 wt. %) and Me6C (6 wt. %) forming eutectic grains. It has been established that the tempering of the deposited layer is accompanied by the pre-transformation of residual austenite with the formation of nanoscale particles of iron and chromium carbides along the boundaries of martensite crystals. Microcracks have been identified along the interfacial interfaces and in the volume of the plates of the carbide phase of eutectic grains, which can initiate the destruction of the deposited layer material during operation.</p></trans-abstract><kwd-group xml:lang="ru"><kwd>быстрорежущая молибденовая сталь</kwd><kwd>наплавка</kwd><kwd>плазменный метод</kwd><kwd>термическая обработка</kwd><kwd>элементный и фазовый состав</kwd><kwd>дефектная субструктура</kwd></kwd-group><kwd-group xml:lang="en"><kwd>high-speed molybdenum steel</kwd><kwd>surfacing</kwd><kwd>plasma method</kwd><kwd>heat treatment</kwd><kwd>elemental and phase composition</kwd><kwd>defective substructure</kwd></kwd-group></article-meta></front><back><ref-list><title>References</title><ref id="cit1"><label>1</label><citation-alternatives><mixed-citation xml:lang="ru">Емелюшин А.Н., Петроченко Е.В., Нефе- дьев С.П. Исследование структуры и ударно- абразивной износостойкости покрытий системы Fe ‒ C ‒ Cr ‒ Mn ‒ Si, дополнительно легированных азотом. Сварочное производство. 2011;10:18‒22.</mixed-citation><mixed-citation xml:lang="en">Emelyushin A.N., Petrochenko E.V., Nefed'ev S.P. Investigation of the structure and impact-abrasive wear resistance of Fe‒C‒Cr‒Mn‒Si system coatings additionally doped with nitrogen. Svarochnoe proizvodstvo. 2011;10:18‒22. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit2"><label>2</label><citation-alternatives><mixed-citation xml:lang="ru">Нефедьев С.П., Емелюшин А.Н. Плазменное упрочнение поверхности. Старый Оскол: ТНТ, 2021;156.</mixed-citation><mixed-citation xml:lang="en">Nefed'ev S.P., Emelyushin A.N. Plasma surface hardening. Staryi Oskol: TNT, 2021;156. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit3"><label>3</label><citation-alternatives><mixed-citation xml:lang="ru">Hacisalihoglu I., Yildiz F., Alsaran A. Wear performance of different nitride-based coatings on plasma nitrided AISI M2 tool steel in dry and lubricated conditions. Wear. 2017;384-385:159–168.</mixed-citation><mixed-citation xml:lang="en">Hacisalihoglu I., Yildiz F., Alsaran A. Wear performance of different nitride-based coatings on plasma nitrided AISI M2 tool steel in dry and lubricated conditions. Wear. 2017;384-385:159–168.</mixed-citation></citation-alternatives></ref><ref id="cit4"><label>4</label><citation-alternatives><mixed-citation xml:lang="ru">Ivanov Yu.F., Gromov V.E., Potekaev A.I., Guseva T.P., Chapaikin A.S., Vashchuk E.S., Romanov D.A. Structure and properties of R18U surfacing of high-speed steel after its high tempering. Russian Physics Journal. 2023;66(7);731‒739. https://doi.org/10.1007/s11182-023-02999-w</mixed-citation><mixed-citation xml:lang="en">Ivanov Yu.F., Gromov V.E., Potekaev A.I., Guseva T.P., Chapaikin A.S., Vashchuk E.S., Romanov D.A. Structure and properties of R18U surfacing of high-speed steel after its high tem-pering. Russian Physics Journal. 2023;66(7);731‒739. https://doi.org/10.1007/s11182-023-02999-w</mixed-citation></citation-alternatives></ref><ref id="cit5"><label>5</label><citation-alternatives><mixed-citation xml:lang="ru">Emelyushin A.N., Petrochenko E.V., Nefed′ev S.P. Inverstigation of the structure and impact-abrasive resistance of coatings of the Fe‒C‒Cr‒Mn‒Si system, additionally alloyed with nitrogen. Welding International. 2013;27(2):150‒153.</mixed-citation><mixed-citation xml:lang="en">Emelyushin A.N., Petrochenko E.V., Nefed′ev S.P. Inverstigation of the structure and impact-abrasive resistance of coatings of the Fe‒C‒Cr‒Mn‒Si system, additionally alloyed with nitro-gen. Welding International. 2013;27(2):150‒153.</mixed-citation></citation-alternatives></ref><ref id="cit6"><label>6</label><citation-alternatives><mixed-citation xml:lang="ru">Kravchenko I.N., Kartsev S.V., Kolomeichen-ko A.V. et al. Metallurgical Features of Plasma Surfacing with Powder Hard Alloy with Addition of Aluminum Powder. Metallurgist. 2021;64(9-10):1077‒1085. https://doi.org/10.1007/s11015-021-01089-x</mixed-citation><mixed-citation xml:lang="en">Kravchenko I.N., Kartsev S.V., Kolomeichenko A.V. et al. Metallurgical Features of Plasma Sur-facing with Powder Hard Alloy with Addition of Aluminum Powder. Metallurgist. 2021;64(9-10):1077‒1085. https://doi.org/10.1007/s11015-021-01089-x</mixed-citation></citation-alternatives></ref><ref id="cit7"><label>7</label><citation-alternatives><mixed-citation xml:lang="ru">Ivanov Yu.F., Gromov V.E., Yuryev A.B., Minenko S.S., Semin A.P., Chapaikin A.S. Structure, Phase Composition, and Surface Properties of R2M9 High-Speed Steel. Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques. 2024;18(6):1395–1400.</mixed-citation><mixed-citation xml:lang="en">Ivanov Yu.F., Gromov V.E., Yuryev A.B., Minenko S.S., Semin A.P., Chapaikin A.S. Structure, Phase Composition, and Surface Properties of R2M9 High-Speed Steel. Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques. 2024;18(6):1395–1400.</mixed-citation></citation-alternatives></ref><ref id="cit8"><label>8</label><citation-alternatives><mixed-citation xml:lang="ru">Кремнев Л.С., Онегина А.К., Виноградова Л.А. Особенности превращений, структуры и свойств молибденовых быстрорежущих сталей. Металловедение и термическая обработка металлов. 2009;12(654):13‒19. EDN: KZSBKP</mixed-citation><mixed-citation xml:lang="en">Kremnev L.S., Onegina A.K., Vinogradova L.A. Peculiarities of transformations, structure and properties of molybdenum high-speed steels. Metallovedenie i termicheskaya obrabotka metal-lov. 2009;12(654):13‒19. (In Russ.). EDN: KZSBKP</mixed-citation></citation-alternatives></ref><ref id="cit9"><label>9</label><citation-alternatives><mixed-citation xml:lang="ru">Кремнев Л.С. Теория легирования и создание на ее основе теплостойких инструментальных сталей и сплавов. МиТОМ. 2008;11:18‒28. EDN: KVXKKF</mixed-citation><mixed-citation xml:lang="en">Kremnev L.S. The theory of alloying and the creation of heat-resistant tool steels and alloys based on it. MiTOM. 2008;11:18‒28. (In Russ.). EDN: KVXKKF</mixed-citation></citation-alternatives></ref><ref id="cit10"><label>10</label><citation-alternatives><mixed-citation xml:lang="ru">Rakhadilov B.K., Wieleba W., Kylyshkanov M.K. et al. Structure and phase composition of high ‒ speed steels. Bulletin of the Karaganda University. Physics Series. 2020;2(98):83‒92. https://doi.org/10.31489/2020Ph2/83-92</mixed-citation><mixed-citation xml:lang="en">Rakhadilov B.K., Wieleba W., Kylyshkanov M.K. et al. Structure and phase composition of high - speed steels. Bulletin of the Karaganda University. Physics Series. 2020;2(98):83‒92. https://doi.org/10.31489/2020Ph2/83-92</mixed-citation></citation-alternatives></ref><ref id="cit11"><label>11</label><citation-alternatives><mixed-citation xml:lang="ru">Иванов Ю.Ф. Структурные и фазовые пре-вращения в ряде сталей при статическом и динамическом режимах термической обра-ботки. Автореферат дис. докт. ф.-м. наук. Москва, 2002:41.</mixed-citation><mixed-citation xml:lang="en">Ivanov Yu.F. Structural and phase transfor-mations in a number of steels under static and dynamic heat treatment conditions. Avtoref. dis. dokt. f.-m. nauk. Moscow, 2002:41. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit12"><label>12</label><citation-alternatives><mixed-citation xml:lang="ru">Модификация поверхности металлических материалов низкоэнергетическими сильно-точными электронными пучками / В.П. Рот-штейн, Д.И. Проскуровский, Г.Е. Озур, Ю.Ф. Иванов. Новосибирск: СО РАН Наука, 2019:348.</mixed-citation><mixed-citation xml:lang="en">Rotshtein V.P., Proskurovskii D.I., Ozur G.E., Ivanov Yu.F. Modification of the surface of me-tallic materials by low-energy high-current elec-tron beams. Novosibirsk: SO RAN Nauka, 2019:348. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit13"><label>13</label><citation-alternatives><mixed-citation xml:lang="ru">Эволюция структуры поверхностного слоя стали, подвергнутой электронно-ионно-плазменной обработке / Под. ред. Н.Н. Кова-ля, Ю.Ф. Иванова. Томск: НТЛ, 2016:298.</mixed-citation><mixed-citation xml:lang="en">Koval' N.N., IvanovYu.F. ed. Evolution of the structure of the surface layer of steel subjected to electron-ion-plasma treatment. Tomsk: NTL, 2016:298. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit14"><label>14</label><citation-alternatives><mixed-citation xml:lang="ru">Модифицирование и легирование поверхности лазерными, ионными и электронными пучка-ми / Под ред. Дж. Поута, Г. Фоти, Д. Дже-кобсона. Москва: Машиностроение, 1987:424.</mixed-citation><mixed-citation xml:lang="en">Pout Dzh., Fot G., Dzhekobson D. ed. Modifica-tion and doping of the surface by laser, ion and electron beams. Moscow: Mashinostroenie, 1987:424. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit15"><label>15</label><citation-alternatives><mixed-citation xml:lang="ru">Иванов Ю.Ф., Громов В.Е., Миненко С.С., Гусева Т.П., Чапайкин А.С., Семин А.П. Структура и свойства поверхностного слоя, полученного плазменной наплавкой из высокоэнтропийной молибденовой быстрорежущей стали, после комплексной обработки. Материаловедение. 2025;6:15‒23.</mixed-citation><mixed-citation xml:lang="en">Ivanov Yu.F., Gromov V.E., Minenko S.S., Guseva T.P., Chapaikin A.S., Semin A.P. Struc-ture and properties of the surface layer obtained by plasma surfacing from high-entropy molyb-denum high-speed steel, after complex pro-cessing. Materialovedenie. 2025;6:15‒23. (In Russ.).</mixed-citation></citation-alternatives></ref><ref id="cit16"><label>16</label><citation-alternatives><mixed-citation xml:lang="ru">Gromov V.E., Ivanov Yu.F., Yuryev A.B., Minenkо S.S., Konovalov S.V. Modification of transition zone structure of high-speed steel sur-facing ‒ substrate by electron-beam treatment. Вестник Сибирского государственного инду-стриального университета. 2025;1(51):43‒50.</mixed-citation><mixed-citation xml:lang="en">Gromov V.E., Ivanov Yu.F., Yuryev A.B., Minenkо S.S., Konovalov S.V. Modification of transition zone structure of high-speed steel sur-facing ‒ substrate by electron-beam treatment. Bulletin of the Siberian State Industrial Universi-ty. 2025;1(51):43‒50.</mixed-citation></citation-alternatives></ref><ref id="cit17"><label>17</label><citation-alternatives><mixed-citation xml:lang="ru">Пайкин А.Г., Шулов В.А., Энгелько В.И. и др. Кратерообразование на поверхности деталей из жаропрочной стали 15Х16К5Н2МВФАВ-Ш при облучении сильноточными импульсными электронными пучками. Упрочняющие технологии и покрытия. 2006;10:9−14. EDN: HVMOZZ.</mixed-citation><mixed-citation xml:lang="en">Paikin A.G., Shulov V.A., Engel'ko V.I. etc. Cratering on the surface of parts made of heat-resistant steel 15X16K5N2MVFAV-Sh when ir-radiated with high-current pulsed electron beams. Uprochnyayushchie tekhnologii i pokrytiya. 2006;10:9−14. (In Russ.). EDN: HVMOZZ.</mixed-citation></citation-alternatives></ref><ref id="cit18"><label>18</label><citation-alternatives><mixed-citation xml:lang="ru">Шулов В.А., Пайкин А.Г., Белов А.Б. и др. Модификация поверхности деталей из жаро-прочных сталей сильноточными импульсны-ми электронными пучками. Физика и химия обработки материалов. 2005;2:61−70. EDN: HSGMVF</mixed-citation><mixed-citation xml:lang="en">Shulov V.A., Paikin A.G., Belov A.B. etc. Modification of the surface of parts made of heat-resistant steels by high-current pulsed electron beams. Fizika i khimiya obrabotki materialov. 2005;2:61−70. (In Russ.). EDN: HSGMVF</mixed-citation></citation-alternatives></ref><ref id="cit19"><label>19</label><citation-alternatives><mixed-citation xml:lang="ru">Fedorov S., Sharipov Ja., Abrorov A. Increasing the surface stability of the cutting tool through complex machining. Journal of Physics: Confer-ence Series: II International Scientific Confer-ence on Metrological Support of Innovative Technologies (ICMSIT II-2021), St. Petersburg, 2021;1889:22079. https://doi.org/10.1088/1742-6596/1889/2/022079</mixed-citation><mixed-citation xml:lang="en">Fedorov S., Sharipov Ja., Abrorov A. Increasing the surface stability of the cutting tool through complex machining. Journal of Physics: Confer-ence Series: II International Scientific Confer-ence on Metrological Support of Innovative Technologies (ICMSIT II-2021), St. Petersburg, 2021;1889:22079. https://doi.org/10.1088/1742-6596/1889/2/022079</mixed-citation></citation-alternatives></ref><ref id="cit20"><label>20</label><citation-alternatives><mixed-citation xml:lang="ru">Egerton F.R. Physical Principles of Electron Mi-croscopy. Basel: Springer International Publish-ing, 2016:196.</mixed-citation><mixed-citation xml:lang="en">Egerton F.R. Physical Principles of Electron Mi-croscopy. Basel: Springer International Publish-ing, 2016:196.</mixed-citation></citation-alternatives></ref><ref id="cit21"><label>21</label><citation-alternatives><mixed-citation xml:lang="ru">Kumar C.S.S.R. Transmission Electron Micros-copy. Characterization of Nanomaterials. New York: Springer, 2014:717.</mixed-citation><mixed-citation xml:lang="en">Kumar C.S.S.R. Transmission Electron Micros-copy. Characterization of Nanomaterials. New York: Springer, 2014:717.</mixed-citation></citation-alternatives></ref><ref id="cit22"><label>22</label><citation-alternatives><mixed-citation xml:lang="ru">Carter C.B., Williams D.B. Transmission Elec-tron Microscopy. Berlin: Springer International Publishing, 2016:518.</mixed-citation><mixed-citation xml:lang="en">Carter C.B., Williams D.B. Transmission Elec-tron Microscopy. Berlin: Springer International Publishing, 2016:518.</mixed-citation></citation-alternatives></ref></ref-list><fn-group><fn fn-type="conflict"><p>The authors declare that there are no conflicts of interest present.</p></fn></fn-group></back></article>
